TURBOMATRIX SERIESTHERMAL DESORBERSUser’s GuideGAS CHROMATOGRAPHY
ContentsviAmbient Pressure Calibration ... 259Checking the Pneumatics for the TurboMatrix Series PPC Units...
Operation92• set and view current configuration parameters (Status tab)• run analyses using one or multiple methods (Run tab)• view instrument informa
Operation
Operation94has been selected, then you only need to enter the tube range. The selected method will be displayed and you will not be able to access the
Operation
Operation96method. The instrument status will be Standby until the instrument reaches all of the set points. If you are using a TD, you must now load
Operation
Operation98The ATD/TD incorporates a packed cold trap to concentrate the volatiles before injection onto the GC column. It is cooled to temperatures b
Operation
Operation100Figure 19 Timing TabThe name of the method that is currently loaded on the Run tab is also displayed. The settings displayed here are from
Operation
Contents
Operation102Enter a Loop Load time. This will determine the time interval that ISV1 is open to load the sample loop in preparation to introducing the
Operation
Operation104Figure 22 Options Tab for a TurboMatrix 150 ATDIf you have the Standard Injection option installed, but do not need to use it, then de-sel
Operation
Operation106is when the sample is purged of residual air at ambient temperature. If you enabled the heated purge option, then the tube will be heated
Operation
Operation108In this mode, only the cold trap is heated and the contents of the trap are desorbed and vented through the Input Split flow control to pr
Operation
Operation110Column Pressure—In the TD/ATD, the Pressure Control system is a manual Pressure Regulator (not a programmable function). Setting a value h
Operation
ContentsviiiNitrogen Flow Rates...392Index ...395
Operation112ToolsPressing the Tools button opens a pop-up menu of tools that enable you to perform various functions such as creating and editing meth
Operation
Operation114Del key to delete the characters.5. Press OK to enter the new name for your method and then press OK to save the method. Press Done to com
Operation
Operation116Maintenance TabYou will use the Maintenance tab to set flows or perform routine maintenance on the instrument. The Maintenance tab contain
Operation
Operation118Figure 28 Preferences Run TabSingle Method Operation—If you select single method operation you can also specify the method to be used. The
Operation
Operation120split on. See Setting the Outlet Split Flow on page 80 for details on setting the outlet split flow.Liquid N2 Option—Check this option to
Operation
ixFiguresFigure 1 The ATD/TD Input/Output (I/O) Port ...43Figure 2 Connecting the Fail Output Signal in Parallel with the Start Si
To enable and use this option:1. Select the Setup tab.2. Press the Password Protection check box. A check mark will appear in the box to enable the op
Operation
Operation124Connect TabKey Clicks— If enabled, this option sounds a tone each time a button is pressed, to confirm that you have pressed a key. Baud R
Operation
Operation126groove, and prying them apart. Other techniques, such as twisting the pen-clip from the tube, can cause permanent damage to the pen-clip.
Operation
Operation128Single Method Operation on the TDOnce you have set up the TD and entered a method for your application you are ready to begin analyzing yo
Operation
Operation130The method can be stopped at any time by pressing the Stop button. A confirmation pop-up window will display, press Ye s to confirm that y
Operation
FiguresxFigure 30 Setup Tab ... 121Figure 31 Password ...
Operation132NOTE: Before powering up the TD/ATD again, ensure thata) Carrier Gas supply and Dry Air to the TD are restored,b) Wait 20 to 30 minutes to
Operation
Operation134and stop tubes. The tube range will default to 1 to 50. Press the first entry box to enable the option. If you are using a TD, the tube ra
Operation
Operation136Editing a SequenceTo delete an entry from the sequence, select the entry in the list and press the Del button. To change the tube range, y
Operation
Operation138Heat Rate—Once the volatiles are transferred from the sample tube, the trap is heated. Set the heating rate to any value between 5, 20, 40
Operation
Operation140Figure 36 Timing TabThe name of the method that is currently loaded on the Run tab is also displayed. The settings displayed here are from
Operation
Figures
Operation142being chromatographed. This setting is intended to ensure that the current run has finished in time for the trap desorption of the next sa
Operation
Operation144Figure 39 Internal Standard Popup for the TurboMatrix 650 ATDThe Options TabThe Options button at the bottom of the Status screen provides
Operation
Operation146Inlet Split and Outlet Split Options—Two split points are provided on the ATD/TD: one before and one after the cold trap. By using either
Operation
Operation148Operating ModesNOTE: The screen above shows operating modes for a TurboMatrix 650 ATD.The ATD/TD can operate in any one of five modes. A b
Operation
Operation150Load Internal Standard (ISTD) on TubeIf the instrument has been equipped with the Internal Standard option, a metered volume of an analyti
Operation
FiguresxiiFigure 101 Open Loop Purging Apparatus with Removable Adsorbent Tube...334Figure 102 S
Operation152Inlet Split- Set the Inlet Split flow rate by accessing the entry field and incrementing or decremented the displayed value with the plus/
Operation
Operation154Pressure or the Trap Desorb Flow Time is set to zero, the system will default to the Isobaric Pressure Injection Mode.To set the Trap Deso
Operation
Operation156also contain the date and time the sequence was started and when the sequence was completed.ToolsPressing the Tools button opens a pop-up
Operation
Operation158complete the selection and return to the Run tab.Activate Command—This command makes the currently selected method active. The method is l
Operation
Operation160Maintenance TabYou will use the Maintenance tab to set flows or perform routine maintenance on the instrument. The Maintenance tab contain
Operation
xiiiTable 1 ATD/TD Shipping Kit...19Table 2 Electrical Protection ...
Operation162Preferences TabYou will use the Preference tab to set the configuration options for the TD. The selections you make here will enable or di
Operation
Operation164Figure 48 Config TabNOTE: Integrity Testing button is grayed out for all models except the TurboMatrix 650 ATD. See the section on Integri
Operation
Operation166Liquid N2 Option-Check this option to enable it on the Status tab. The option allows you to cool the cold trap down to -100°C. This option
Operation
Operation168Monitor Trap Impedance-Selection of the check box enables the input boxes for Lower and Upper Limits. The measured pressure will be report
Operation
Operation170Protection” and the pop-up Password box will appear in the figure above. If you wish to create a new password, touch each box and the alph
Operation
TablesxivTable 34 Column (0.32 mm) Flow Rates with Helium Carrier Gas ...389Table 35 Column (0.53 mm) Fl
Operation172Connect TabKey Clicks— If enabled, this option sounds a tone each time a button is pressed, to confirm that you have pressed a key. Baud R
Operation
Operation174The pen-clip can be removed from a sample tube by inserting a wide-bladed screwdriver between the clip and the tube, close to the groove,
Operation
Operation176tab.3. If you are running with a pre-selected method you only need to load the tube. 4. If the method has not been selected, select it now
Operation
Operation1783. Enter the desired end tube.4. From the method drop-down box, select the method to be used for the selected range of tubes.5. Press the
Operation
Operation180
Accessories 4
Introduction 1
Accessories
Accessories184window.8. If you are using the Method Editor, save your method. If you are using the Status tab, you must enter all of the other method
Accessories
Accessories186Tubes and CapsThe ATD/TD uses industry standard, patented stainless steel tubes. The stainless steel tubes are compatible with pumped an
Accessories
Accessories188Capped Sample Tubes (with PTFE Analysis Caps)Stainless SteelGlass Glass Lined Stainless SteelQtyM041-3595 M041-3598 M041-3597 10M041-359
Accessories
Accessories190(140 to180 kPa).To conserve liquid nitrogen, the accessory will be turned off automatically under the following conditions: • when the A
Accessories
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Accessories192Figure 59 Flow Diagram of the TurboMatrix 350 ATD (PPC) with Internal Standard Accessory The standard addition accessory is kept at ambi
Accessories
Accessories1944. 4. In the same dialog box you can set the Inject Time (in minutes) to the amount of time you want helium to go through the loop onto
Accessories
Accessories196upon and set.This function is available by selecting the Preferences entry on the Tools menu and then selecting the Config tab and the I
Accessories
NOTE: Use a clean sample tube that does not contain a sample for the set-up procedure. The sample tube should contain the type of packing material tha
Accessories
Accessories200Figure 61 Sequential Tube Sampler with monitoring pump.Contact PerkinElmer for further details about this accessory. Online Sampling Acc
Accessories
Introduction
Accessories202
Method Development 5
Method Development
Method Development206The process of developing thermal desorption methods can be greatly simplified by keeping the principles given below in mind when
Method Development
Method Development208Setting System ParametersTemperature TabThere are five temperature settings for the TD: tube oven temperature, the transfer line
Method Development
Method Development210time but may be required for the analysis of thermally labile analytes.Trap High Temperature—The trap is heated to the high tempe
Method Development
Introduction14TurboMatrix 100 TD: Single-tube, manual-pneumatics model, can be upgraded to the automated version. Also includes a separate trap-clean-
Method Development212overlapping tube desorptions and analyses to maximize throughout. For example, if the CYCLE TIME is 42 minutes after the previous
Method Development
Method Development214If you have enabled this option, then you must enter a Standard Inject time on the Timing tab. The standard addition valve is act
Method Development
Method Development216degrade rapidly and leak. You may also want to install high temperature o-rings into the fixed seal assembly. The high temperatur
Method Development
Method Development218Upon completion of each flow adjustment an entry of its value can be made in the respective field of the Status/Pnu tab. These se
Method Development
Method Development220Carbotrap™Carbopack B ™(n-C4) n-C5 to n-C14400 100 Wide range of VOCs including ketones, alcohols and aldehydes (bp>75°C), and
Method Development
Introduction
Method Development222temperatures, up to 300°C and more, for efficient thermal desorption.1As a general policy it is a good idea to use similar sorben
Method Development
Method Development224Compound Boiling Point (°C) Retention Volume at 20 °C (l/g)Heptane 98 170Octane 125 780*Benzene 80 62Toluene 111 360Xylenes 138-1
Method Development
Method Development226Figure 65 Glass or Stainless Steel Sample Tubes Containing Adsorbents of Increasing Strength Linked Together in Series In this ca
Method Development
Method Development228All forms of Tenax are susceptible to decomposition since they are polymer based, so there is always some background (artifacts)
Method Development
Method Development230your trap loading and column capacity and flow, figure out how much sample you need on the trap and therefore what the outlet spl
Method Development
Introduction16About this ManualThis manual is an integral part of your thermal desorber. It begins with unpacking and general safety information in Ch
Method Development232 Outlet Split = 8 mL/minIn the above example, the trap desorption flow of 10/mL/min is barely suffic
Method Development
Method Development234The percentage of components from the sampling tube which reach the analytical column is:Equation 10Example: In this example 10%
Method Development
Method Development236Four major techniques are commonly used to introduce standards into desorption tubes.Vaporizing a Liquid StandardIn the first met
Method Development
Method Development238Internal Standard Addition AccessoryThe Internal Standard Addition accessory is required for the third method. A gaseous calibrat
Method Development
Method Development240Desorb-Rec-Same: This method will inject a sample but instead of loosing the sample to outlet split the split flow is directed to
Routine Maintenance 6
Introduction
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Routine Maintenance
Routine Maintenance244Table 17 Maintenance ScheduleCleaning the InstrumentExterior surfaces may be cleaned with a soft cloth, dampened with a mild de
Routine Maintenance
Routine Maintenance246Sample Tubes and Storage CapsWhen samples have been collected, the tubes should be analyzed as soon as possible. If the tubes ca
Routine Maintenance
Routine Maintenance248Figure 69 ATD Arm HousingTo gain access to the top of the heated valve, you must further remove the transfer line cover.8. Remov
Routine Maintenance
Routine Maintenance250and 0920-0093) are intended for operation up to 300 °C. See High Temperature Operation on page 215 for further details.We recomm
Routine Maintenance
Introduction18the side.3. Lift out the instrument using the two lifting straps.4. Check that all ordered parts have been supplied undamaged.The follow
Routine Maintenance252NOTE: Do not over tighten the seal.Table 18 Fixed and Mobile Seal Replacement O-RingsChanging the O-Rings and Filter Disk in th
Routine Maintenance
Routine Maintenance2544. Remove the carousel and bottom cover.Figure 71 Automated Mobile Seal5. Turn the mobile seal cap counterclockwise to remove it
Routine Maintenance
Routine Maintenance256inserting the end of the column into a silicone septum. 1/8” packed columns may be capped using a 1/8” Swagelok® cap (P/N 0496-7
Routine Maintenance
Routine Maintenance258select Maintenance and select Column Leak Test. The following screen will appear. Press OK to start the test.If your GC fails th
Routine Maintenance
Routine Maintenance260Checking the Pneumatics for the TurboMatrix Series PPC UnitsYou may need to check the pneumatics on the three available units wi
Routine Maintenance
Introduction
Routine Maintenance262Where: Fa is the measured flow rate under ambient conditions (mL/min). Fs is the flow rate entered/display
Routine Maintenance
Routine Maintenance2644. Set the Valve temperature to the value required for the analysis. NOTE: For the best accuracy, the calibration procedure shou
Routine Maintenance
Routine Maintenance2666. Place a clean and empty glass or stainless steel tube into Position 1 (see the following figure) of the carousel and press th
Routine Maintenance
Routine Maintenance2688. Manually transpose the average Actual values into the corresponding Offset fields.
Routine Maintenance
Routine Maintenance270Removing the Cold TrapNOTE: Always have one or two spare traps on hand in case of breakage before proceeding.To remove the cold
Routine Maintenance
Introduction20Symbols Used on the InstrumentFurther information is available in this safety section.Safety InformationThis manual contains information
Routine Maintenance272Figure 76 Cold Trap8. Remove the Desorb line and slide it to the back. See the following figure.CAUTIONBefore shutting off both
Routine Maintenance
Routine Maintenance27410. Carefully remove the o-ring from the trap by removing the nut and removing the brass ring. See the following figure.Figure 7
Routine Maintenance
Routine Maintenance2762. Also on the left side of the trap, reattach the brass nut and tighten. Figure 81 Trap O-Ring, Brass Ring and Nut 3. Put the
Routine Maintenance
Routine Maintenance278When specifying a Trap Clean method in a sequence, the method must have a tube assigned to it. An empty tube is best suited for
Routine Maintenance
Routine Maintenance2802. Using the cold trap packing tool (P/N L427-1203), remove the old packing. Insert the tool into the cold trap and gently push
Routine Maintenance
Introduction
Routine Maintenance282Under normal operating conditions, the filter disks do not require changing. However, they must be changed if the packing of the
Routine Maintenance
Routine Maintenance28413. Connect the supply of purge air and carrier gas and begin purging the cold trap enclosure. Wait for 30 minutes before poweri
Routine Maintenance
Routine Maintenance286When tubes are packed with more than one adsorbent in series, the different beds of packing are usually separated with glass woo
Routine Maintenance
Routine Maintenance288conditioning stages until it is finally close to, or at, the maximum temperature limit for the packing material. Where possible,
Routine Maintenance
Routine Maintenance290Once the packed tubes have been thoroughly conditioned in this way, subsequent conditioning runs (for example, after storage) wo
Routine Maintenance
TurboMatrix Series Thermal DesorbersUser’s Guide
Introduction22.Line Cord—Use only approved line cords with a protective ground conductor (green or green/yellow) to ensure safe operation. The line co
Routine Maintenance292To replace fuses:1. Ensure that the power cord is disconnected from the power entry module on the rear left side of the instrume
Routine Maintenance
Routine Maintenance294
Theory of Thermal Desorption 7
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Theory of Thermal Desorption
Theory of Thermal Desorption298or decrease the carrier-gas pressure during trap desorption to improve desorption efficiency and give better recoveries
Theory of Thermal Desorption
Theory of Thermal Desorption300Figure 86 Standby ConfigurationNOTE: SV is a solenoid valve, and PR is a pressure regulator in this section.In standby,
Theory of Thermal Desorption
Introduction
Theory of Thermal Desorption302Start of the Tube Conditioning Sequence—When the tube conditioning sequence is started, the carrier gas pressure is tes
Theory of Thermal Desorption
Theory of Thermal Desorption304Upon finishing the leak test, SV1 and SV3 open and the sample tube is purged with carrier gas for the duration of the p
Theory of Thermal Desorption
Theory of Thermal Desorption306If SV4 is open, it will remain open for the three minutes and switch with SV2. SV2 and SV4 (if selected) will switch th
Theory of Thermal Desorption
Theory of Thermal Desorption308Figure 90 Pressurize Sample TubePrimary and Secondary Leak Test of the Sample TubeIf no large leaks are detected, SV1 i
Theory of Thermal Desorption
Theory of Thermal Desorption310The number of retries can be set to between zero and two (0-2); the default value is two (with two retries, a total of
Theory of Thermal Desorption
Introduction24Mechanical HazardWhen working with the instrument, please observe the following:• Keep your hands, clothing and other objects away from
Theory of Thermal Desorption312adsorbent to strong adsorbent. Any volatiles purged out of the weak adsorbent will land on the strong adsorbent (see th
Theory of Thermal Desorption
Theory of Thermal Desorption314Single-Stage versus Two-Stage DesorptionSingle Stage (Non-PerkinElmer)If the volatiles extracted from the sample by the
Theory of Thermal Desorption
Theory of Thermal Desorption316in the environmental field where samples frequently contain a significant amount of water.Packed cold traps can functio
Theory of Thermal Desorption
Theory of Thermal Desorption318
Sampling Techniques 8
Sampling Techniques
Introduction
Sampling Techniques322Figure 96 Principles of Diffusive SamplingUnder these conditions, components will migrate to the adsorbent or reactive surface a
Sampling Techniques
Sampling Techniques324If the concentration is required in ppm, then the formula is modified to include the molecular weight of the compound of interes
Sampling Techniques
Sampling Techniques326Alternatively, the uptake rate can be determined experimentally. One quick experiment that can be used either to determine appro
Sampling Techniques
Sampling Techniques328placed over the front of the tube to reduce the ingress of particulate material if required. (P/N L407-0208)The flow rate range
Sampling Techniques
Sampling Techniques330Table 25 Mass of Component Collected on a Sample TubeDuring Pumped Air Monitoring The data in Table 26 is based on a sampling t
Sampling Techniques
Introduction26• Do not heat the cylinders or expose them to direct sunlight. The cylinders may rupture at high temperatures.• Do not mutilate cylinder
Sampling Techniques332obtained from regular monitoring for individual analytes will vary considerably.Figure 99 Probability of a Result Occurring vers
Sampling Techniques
Sampling Techniques334Purge and TrapOne of the variations of vapor phase sampling is the purge and trap technique. In this method, an inert gas is use
Sampling Techniques
Sampling Techniques336Table 28 GC Certified Standards on PerkinElmer TubesThese analytical results were in agreement with the values calculated from
Sampling Techniques
Sampling Techniques338Figure 104 Sampling Resins and Ointments Sampling SolidsIdeal solids for analysis by thermal desorption have a large surface are
Sampling Techniques
Sampling Techniques340If a 1 µL injection of standard solution is to be used, the concentration of the solution must be approximately 25% by volume. 1
Troubleshooting 9
Introduction
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Troubleshooting
Troubleshooting344Status DescriptionEconomy Mode The instrument is in the economy mode. The heaters have been switched off and the carrier gas flow ha
Troubleshooting
Troubleshooting346Status DescriptionARM TO DECAPPERContact your PerkinElmer Service Representative if you get this message.ARM TO DESORBContact your P
Troubleshooting
Troubleshooting348Status DescriptionDECAPPER CLOSECheck the air pressure, the valve could be leaking or failing, check for a mechanical obstruction. I
Troubleshooting
Troubleshooting350Status DescriptionOVEN FAIL AT IDLE POSITIONContact your PerkinElmer Service Representative if you get this message.OVEN FAIL AT TUB
Troubleshooting
• Secure the Dewar vessel so that it cannot fall over. • Protect the Dewar vessel from any damage and from sources of heat. The Dewar vessel must be f
Troubleshooting352Table 30 TurboMatrix Status and Error Messages SummaryInstrument Fault ConditionsIf there is more than one fault occurring at a tim
Troubleshooting
Troubleshooting354Fault: Carousel Motor StalledCause: An obstruction has caused the carousel to halt rotation.Action: Turn the ATD off and disconnec
Troubleshooting
Troubleshooting356the gripper arm has dropped a tube.Action: Turn the ATD off and disconnect the power cord from the AC mains. Remove the case as out
Troubleshooting
Troubleshooting358Action: Ensure nothing is touching the carousel. Action: Ensure all of your tubes have been installed correctly. If pen clips are
Troubleshooting
Troubleshooting360Re-orient the tube on the carousel. Touch the Tools button, press Reset in the menu and answer Yes to the pop-up question.The instr
Troubleshooting
Introduction
Troubleshooting362must be inserted into the carousel with the pen clip facing in, toward the center of the carousel. Re-orient the tube on the carouse
Troubleshooting
Troubleshooting364Fault: Valco-A, B, C or D Valve FailedCause: A Valco valve cannot be initialized. Valco valve A is the heated valve used for normal
Troubleshooting
Troubleshooting366should be replaced as described in Installing the Heated Transfer Line on page 51.Cause: A poor connection between the transfer lin
Troubleshooting
Troubleshooting368Cause: There is ice forming on the cold trap. Action: De-ice the trap as outlined in De-Icing the Cold Trap on page 278. Ensure th
Troubleshooting
Troubleshooting370matrix is not escaping from the tube or trap and migrating into the rest of the system. Use glass wool plugs in the tubes and trap,
Troubleshooting
Introduction30A label with a crossed-out wheeled bin symbol and a rectangular bar indicates that the product is covered by the Waste Electrical and El
Troubleshooting372diffuse back into the system if the filters become overloaded.Action: The inlet and outlet split and desorb charcoal filters must b
Troubleshooting
Troubleshooting374The following conditions are particularly important:• at least 10 mL/min flow is passing through the tube during primary desorption•
Troubleshooting
Troubleshooting376Discrimination of Compounds Over a Wide Boiling RangeCause: The packing material contained in the trap or in the sample tube is not
Troubleshooting
Troubleshooting378
Appendices 10
Appendices
Installation and Setup 2
Appendices382Appendix B Warranty Exclusions and LimitationsThe following consumable items are excluded from your instrument warranty agreement:• Fused
Appendices
Appendices384A Method for the Determination of Personal Exposure to Atmospheric Nitrous Oxide...TDA-17 D
Appendices
Appendices386International Standard Methods Relating to VOC Air Monitoring using Thermal Desorption... GCA-77Bibliography
Appendices
Appendices388Appendix D Carrier Gas PressuresThe flow rates listed below are approximations only. In order to accurately determine the column flow rat
Appendices
Appendices390Table 35 Column (0.53 mm) Flow Rates with Helium Carrier GasHydrogen Flow RatesTable 36 Column (0.22 mm) Flow Rates with Hydrogen Carri
Appendices
Release HistoryUser AssistancePerkinElmer, Inc.710 Bridgeport AvenueShelton CT 06484-4794email: [email protected] information contained i
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Appendices392Table 39 Column (0.53 mm) Flow Rates with Hydrogen Carrier GasNitrogen Flow RatesTable 40 Column (0.22 mm) Flow Rates with Nitrogen Car
Appendices
Table 43 Column (0.53 mm) Flow Rates with Nitrogen Carrier GasNitrogen Flow Rates (mL/min)Column Diameter: 0.53 mm Optimum Flow: 0.79 ml/minInletPres
395IndexAAC Line Connections 40Accessory 200BCD Kit 186Caps 186Gauze-Loading 286Internal Standard 104, 145, 191, 213Liquid Nitrogen (LN2) 189STS-25 19
Index396BBackflush Configuration 281Baud Rate 124, 172BCDData Logic 185Bend Dimensions of Transfer Line 56Benzene, Sampling 328Binary Coded Decimals (
Index398ComplianceEMC Directives 23FCC 23CompoundsSafety Information 24Sampling Emulsions, Liquids 337Sampling Resins, Ointments 338Sampling Solids 33
Index
Index400No Tubes in First-Last 356Oven Fail at Cool Position 362Oven Fail at Idle Position 362Oven Fail at Tube Position 361Robot Arm 354Sealer Fail a
Installation and Setup
Index402GC 47TD/ATD to HP6890 GC 49Transfer Line 51Tubing Requirements 71InstrumentContamination 370Dimensions 37Fault Conditions 352Input Signals 46L
Index
Index404In this Manual 16Number of Injections 105, 146, 213OOintments, Sampling 338Open Command 113, 157Open Loop Purging 334Operation 85Double Split
Index
Index406Purge Time 100, 140RRate, Heat 98, 138, 209ReadyIn Signal 46Out Signal 43Ready/StartCable Assembly 47HP6890 Cable Assembly 49Redesorbing 339Re
Index
Index408Contacting 381Customer 381SettingAnalysis Options 103, 144Analysis Temperatures 97, 136Analysis Times 99, 139Carrier Gas Flow Rates 77Date 125
Index
Index410Calculator 115, 158Exit Method Editor 114, 158Log Out 158Reset Command 115Tools Menumaintenance options 160Touch ScreenBrightness 124, 172Inte
Index
Installation and Setup34Operating Environment on page 35. 2. Read in Safety in the Introduction chapter and ensure that you have complied with the req
PerkinElmer Life and Analytical Sciences710 Bridgeport AvenueShelton, CT 06484-4794, U.S.A.Internet: http://www.perkinelmer.comemail: info@perkinelmer
Installation and Setup
Installation and Setup36Table 5 Required Laboratory ConditionsAltitude(operating)Sea level (0 metres) to 2000 m (6,562 feet)Storage(non-operating)You
Installation and Setup
Installation and Setup38Allow at least 94 cm (3’) on either side of the TD/GC to accommodate additional equipment (for example, the computer).The labo
Installation and Setup
Installation and Setup40It should be checked by a qualified electrician before you connect the instrument.To avoid interference caused by ground loops
Installation and Setup
iContentsIntroduction ...11Introduction...
Installation and Setup42injector or detector port at the top can be used. This may be the case if you have an older GC or a GC equipped with PPC. Anot
Installation and Setup
Installation and Setup44The contacts remain closed for 6 seconds. The Start signal is normally used to start a GC run, by connecting it to the GC Star
Installation and Setup
Installation and Setup46The Fail signal can be generated at a number of points in the sequence, including detection of an empty tube position or an er
Installation and Setup
Installation and Setup48Connect the opposite end to the GC EXT START pins 3 and 4.Figure 3 Connecting the ATD/TD to the AutoSystem XL GC using the Rea
Installation and Setup
Installation and Setup502. Locate the I/O port on the rear panel of the ATD/TD.3. Connect the white wire of the cable assembly (P/N N610-0402) to the
Installation and Setup
ContentsiiInstalling the Heated Transfer Line... 51Capillary Analytical Column Directly connected to the TD...
Installation and Setup52Figure 5 Installing the Transfer Line on the AutoSystem XLCAUTIONThe stationary phase of your column must be able to withstand
Installation and Setup
Installation and Setup54back of the oven outer wall should be visible. See Figure 9.6. Remove both of the PVC end caps from the oven entry insulation
Installation and Setup
Installation and Setup56Figure 7 Bend Dimensions for Connecting the ATD/TD Transfer Line to an AutoSystem GC or Clarus 500 GC 4. Remove the cap from t
Installation and Setup
Installation and Setup589. From the GC end, pass the fused silica transfer line, or the front end of the GC column (as you prefer), through the instal
Installation and Setup
Installation and Setup60Figure 8 Connect the Transfer Line to the TD Instrument Vespel FerruleGraphitzed Vespel FerruleStainless SteelSleeveHeatedValv
Installation and Setup
Contents
Installation and Setup62Figure 9 Installation of the Transfer Line through the Rear Panel 2. Install a union (P/N 0497-2073 for capillary columns or P
Installation and Setup
Installation and Setup64are not included in the kit.We recommend that you use the 0.53mm ID Retention Gap kit, Part No. 0497-8449.Installing the Trans
Installation and Setup
Installation and Setup66(35 kPa), better carrier gas control can be achieved by inserting a length of narrow bore, fused silica tubing, between the co
Installation and Setup
Installation and Setup680497-2066) or the graphite ferrule supplied with the union (not for ECD or MS). After passing the column end through the ferru
Installation and Setup
Installation and Setup70should be installed at every gas line connection. The carrier gas connections require 1/8” tubing with 1/8” parallel compressi
Installation and Setup
ContentsivRun Tab ...162Config Tab...
Installation and Setup72Use only carrier gases with a purity of 99.995% or better. Only top quality gases are suitable; typical laboratory supplies ar
Installation and Setup
Installation and Setup74compression fitting with which to connect the regulator to the TD. The delivery pressure must be adjustable to 90 psig (620 kP
Installation and Setup
Installation and Setup76Column Leak Test1. To perform the column leak test, cap one end of the column and/or transfer line with a rubber septa. Connec
Installation and Setup
Connect the gas supply line to the carrier in port on the rear panel of the TD. 1. Ensure the transfer line has been connected correctly to the GC. Se
Installation and Setup
Installation and Setup807. Allow a few minutes for the flow to stabilize before disconnecting the flow meter.8. To set the desorb flow, connect a flow
Installation and Setup
Contents
Installation and Setup82
Operation 3
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Operation
Operation86TurboMatrix 350 ATD: Automated sampling of up to 50 tubes, incorporating PPC. Supports pressure, flow and velocity control of the carrier g
Operation
Operation88Attention:Before attempting to disconnect the TD/ATD from the GC or to shut off the carrier gas supply, ensure that:• The GC oven and detec
Operation
Operation90Figure 16 Dimensions of the Automated Thermal Desorber (example shown here is the TurboMatrix Series 300 TD) To begin operation of the ATD
Operation
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