ATD Tools 5928 Handbücher

Bedienungsanleitungen und Benutzerhandbücher für Fernbedingungen ATD Tools 5928.
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Atd tools 5928 Betriebsanweisung (422 Seiten)


Marke: Atd-tools | Kategorie: Fernbedingungen | Größe: 4.33 MB |

 

Inhaltsverzeichnis

TURBOMATRIX SERIES

1

THERMAL DESORBERS

1

TurboMatrix Series

3

Thermal Desorbers

3

User’s Guide

3

M041-3331 E January 2007

4

Contents

10

Introduction 1

19

Introduction

21

About this Manual

24

Unpacking the Instrument

25

Safety Information

28

Electrical Safety

29

Mechanical Hazard

32

Chemicals

32

Handling Compressed Gases

33

Extreme Temperatures

35

Waste Disposal

36

Sample Tubes

36

Products

37

Installation and Setup 2

39

Pre-installation Checklist

41

Installation and Setup

42

Laboratory Requirements

43

Electrical Connections

47

Electrical Surge

48

Chromatograph

49

The ATD/TD Input/Output Port

51

TD Output Signals

51

TurboMatrix I/O Port

53

ATD/TD Input Signals

54

Timed Event Relays

55

Connecting the ATD/TD to the

55

TURBOMATRIX

56

HP 5890 and HP 6890

57

Transfer Line

63

Access Hole

63

Installation at the ATD/TD

65

Panel of the GC

69

Bad Cuts

71

Good Cut

71

Connecting a Packed Column

74

Column to the TD

76

Gas Supply Specifications

78

Gas Connections

79

Carrier In

83

Supply Pressure

83

90 psi/620 kPa

83

Standard In

83

Dry Air In

83

Connecting the Dryer Assembly

84

Setting the Carrier Gas Flows

85

Series 100 TD and 150 ATD

86

Operation 3

91

Attention:

96

Operation

100

100 TD and 150 ATD

101

Creating a Sequence

102

Editing a Sequence

104

Status Tab

104

Temperature Tab

105

Timing Tab

107

The Options Tab

111

Operating Modes

115

Pneumatics Tab

117

The Log Tab

118

Method Editor

120

Preferences

123

Calculator

123

Maintenance Tab

124

Preferences Tab

125

Config Tab

127

Setup Tab

128

Connect Tab

132

Loading Tubes

133

Shutdown

139

Status Line

140

The Run Tab

141

Loading the ATD Carousel

181

Accessories 4

189

<>

190

Options Board

191

Accessories

192

BCD Interface

193

Tubes and Caps

194

Internal Standard Accessory

199

Principle of Operation

201

Operation of the IS Accessory

201

Setting the IS Flow Rates

203

TD Control Software

207

Online Sampling Accessory

208

AutoSystem XL or

209

Clarus 500 GC

209

Method Development 5

211

Method Development

213

Analytical Objectives

213

Setting System Parameters

216

High Temperature Operation

223

Carrier Gas Flow Rates

224

Phase Sampling

226

*Pyridine 116 78

233

Aniline 184 2200

233

Setting Sample Split Ratios

236

Single Split Operation

238

SplitOutlet 2

239

Double-Split Operation

240

Vaporizing a Liquid Standard

244

Sample Tube

245

Atmosphere

246

Sample Integrity Testing

247

Sample Archiving

247

Routine Maintenance 6

249

Routine Maintenance

251

Cleaning the Instrument

252

Cleaning and Decontamination

252

Carrier Gas

253

Adsorbent Storage

253

Sample Tubes and Storage Caps

254

Spectrometer

254

Covers of the ATD

255

Loosen Screw

256

(Do not remove the screw)

256

Remove Screw

256

Door Latch

256

Mobile Seals

257

TD Mobile Seal

260

ATD Mobile Seal

261

Leak Testing

263

Standard Leak Test

265

Impedance Calibration

265

Column Leak Test

265

GC Temp Calib

266

Ambient Pressure Calibration

267

TurboMatrix Series PPC Units

268

Figure 73 Filter in Place

271

Removing the Cold Trap

278

Replacing the Cold Trap

283

Cold Trap Maintenance

285

De-Icing the Cold Trap

286

Repacking the Cold Trap

287

DesorbAdsorb

288

Packing Sample Tubes

292

Stainless Steel Tubes

293

Gauze-Loading Accessory

294

Changing the Fuse

299

Cleaning the ATD Sample Tray

299

Figure 84 Replacing the Fuse

301

Theory of Thermal Desorption

306

Modes of Operation

307

Trap Clean Mode

309

Tube Conditioning

309

Analysis

311

Overlapping Tube Desorption

314

Automated Leak Testing

315

Leak Testing the Cold Trap

317

Number of Leak Test Retries

317

Cold Trap Flow Configuration

321

Desorption

322

Techniques

325

Sampling Techniques 8

327

Sampling Techniques

330

(min) timesamplingx U

331

)(mg/m conc

331

Zx 24.45

332

Analyte Mass

337

Molecular

338

Component

338

Atmospheric

339

Concentration

339

1/3 of the limit

341

Purge and Trap

342

Soil Probes

342

Sampling Resins and Ointments

345

Sampling Solids

346

Troubleshooting 9

349

Troubleshooting

351

Status Messages

351

Instrument Fault Conditions

360

Fatal Errors

372

Edition, (Glasgow, 1996), p27

373

The Cold Trap Does Not Cool

375

Sample Carryover

376

System Contamination

378

Wide Boiling Range

384

Appendices 10

387

Appendix A Customer Service

389

Limitations

390

Appendix C References

391

Appendices

392

Helium Flow Rates

396

Hydrogen Flow Rates

398

Nitrogen Flow Rates

400

710 Bridgeport Avenue

422