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- Inhaltsverzeichnis
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- TURBOMATRIX SERIES 1
- THERMAL DESORBERS 1
- TurboMatrix Series 3
- Thermal Desorbers 3
- User’s Guide 3
- M041-3331 E January 2007 4
- Contents 10
- Introduction 1 19
- Introduction 21
- About this Manual 24
- Unpacking the Instrument 25
- Safety Information 28
- Electrical Safety 29
- Mechanical Hazard 32
- Chemicals 32
- Handling Compressed Gases 33
- Extreme Temperatures 35
- Waste Disposal 36
- Sample Tubes 36
- Products 37
- Installation and Setup 2 39
- Pre-installation Checklist 41
- Installation and Setup 42
- Laboratory Requirements 43
- Electrical Connections 47
- Electrical Surge 48
- Chromatograph 49
- The ATD/TD Input/Output Port 51
- TD Output Signals 51
- TurboMatrix I/O Port 53
- ATD/TD Input Signals 54
- Timed Event Relays 55
- Connecting the ATD/TD to the 55
- TURBOMATRIX 56
- HP 5890 and HP 6890 57
- Transfer Line 63
- Access Hole 63
- Installation at the ATD/TD 65
- Panel of the GC 69
- Bad Cuts 71
- Good Cut 71
- Connecting a Packed Column 74
- Column to the TD 76
- Gas Supply Specifications 78
- Gas Connections 79
- Carrier In 83
- Supply Pressure 83
- 90 psi/620 kPa 83
- Standard In 83
- Dry Air In 83
- Connecting the Dryer Assembly 84
- Setting the Carrier Gas Flows 85
- Series 100 TD and 150 ATD 86
- Operation 3 91
- Attention: 96
- Operation 100
- 100 TD and 150 ATD 101
- Creating a Sequence 102
- Editing a Sequence 104
- Status Tab 104
- Temperature Tab 105
- Timing Tab 107
- The Options Tab 111
- Operating Modes 115
- Pneumatics Tab 117
- The Log Tab 118
- Method Editor 120
- Preferences 123
- Calculator 123
- Maintenance Tab 124
- Preferences Tab 125
- Config Tab 127
- Setup Tab 128
- Connect Tab 132
- Loading Tubes 133
- Shutdown 139
- Status Line 140
- The Run Tab 141
- Loading the ATD Carousel 181
- Accessories 4 189
- <> 190
- Options Board 191
- Accessories 192
- BCD Interface 193
- Tubes and Caps 194
- Internal Standard Accessory 199
- Principle of Operation 201
- Operation of the IS Accessory 201
- Setting the IS Flow Rates 203
- TD Control Software 207
- Online Sampling Accessory 208
- AutoSystem XL or 209
- Clarus 500 GC 209
- Method Development 5 211
- Method Development 213
- Analytical Objectives 213
- Setting System Parameters 216
- High Temperature Operation 223
- Carrier Gas Flow Rates 224
- Phase Sampling 226
- *Pyridine 116 78 233
- Aniline 184 2200 233
- Setting Sample Split Ratios 236
- Single Split Operation 238
- SplitOutlet 2 239
- Double-Split Operation 240
- Vaporizing a Liquid Standard 244
- Sample Tube 245
- Atmosphere 246
- Sample Integrity Testing 247
- Sample Archiving 247
- Routine Maintenance 6 249
- Routine Maintenance 251
- Cleaning the Instrument 252
- Cleaning and Decontamination 252
- Carrier Gas 253
- Adsorbent Storage 253
- Sample Tubes and Storage Caps 254
- Spectrometer 254
- Covers of the ATD 255
- Loosen Screw 256
- (Do not remove the screw) 256
- Remove Screw 256
- Door Latch 256
- Mobile Seals 257
- TD Mobile Seal 260
- ATD Mobile Seal 261
- Leak Testing 263
- Standard Leak Test 265
- Impedance Calibration 265
- Column Leak Test 265
- GC Temp Calib 266
- Ambient Pressure Calibration 267
- TurboMatrix Series PPC Units 268
- Figure 73 Filter in Place 271
- Removing the Cold Trap 278
- Replacing the Cold Trap 283
- Cold Trap Maintenance 285
- De-Icing the Cold Trap 286
- Repacking the Cold Trap 287
- DesorbAdsorb 288
- Packing Sample Tubes 292
- Stainless Steel Tubes 293
- Gauze-Loading Accessory 294
- Changing the Fuse 299
- Cleaning the ATD Sample Tray 299
- Figure 84 Replacing the Fuse 301
- Theory of Thermal Desorption 306
- Modes of Operation 307
- Trap Clean Mode 309
- Tube Conditioning 309
- Analysis 311
- Overlapping Tube Desorption 314
- Automated Leak Testing 315
- Leak Testing the Cold Trap 317
- Number of Leak Test Retries 317
- Cold Trap Flow Configuration 321
- Desorption 322
- Techniques 325
- Sampling Techniques 8 327
- Sampling Techniques 330
- (min) timesamplingx U 331
- )(mg/m conc 331
- Zx 24.45 332
- Analyte Mass 337
- Molecular 338
- Component 338
- Atmospheric 339
- Concentration 339
- 1/3 of the limit 341
- Purge and Trap 342
- Soil Probes 342
- Sampling Resins and Ointments 345
- Sampling Solids 346
- Troubleshooting 9 349
- Troubleshooting 351
- Status Messages 351
- Instrument Fault Conditions 360
- Fatal Errors 372
- Edition, (Glasgow, 1996), p27 373
- The Cold Trap Does Not Cool 375
- Sample Carryover 376
- System Contamination 378
- Wide Boiling Range 384
- Appendices 10 387
- Appendix A Customer Service 389
- Limitations 390
- Appendix C References 391
- Appendices 392
- Helium Flow Rates 396
- Hydrogen Flow Rates 398
- Nitrogen Flow Rates 400
- 710 Bridgeport Avenue 422
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